Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing

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Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing (en)
0-3D наноструктуре за примену у електроници и обновљивим изворима енергије: синтеза, карактеризација и процесирање (sr)
0-3D nanostrukture za primenu u elektronici i obnovljivim izvorima energije: sinteza, karakterizacija i procesiranje (sr_RS)
Authors

Publications

Structure, morphology and photocatalytic properties of CoxMg1-xFe2O4 (0<x<1) spinel ferrites obtained by sol-gel synthesis

Vasiljević, Zorka Ž.; Dojčinović, Milena; Pavlović, Vera P.; Vujančević, Jelena; Tadić, Nenad; Nikolić, Maria Vesna

(Belgrade : Materials Research Society of Serbia, 2019)

TY  - CONF
AU  - Vasiljević, Zorka Ž.
AU  - Dojčinović, Milena
AU  - Pavlović, Vera P.
AU  - Vujančević, Jelena
AU  - Tadić, Nenad
AU  - Nikolić, Maria Vesna
PY  - 2019
UR  - https://machinery.mas.bg.ac.rs/handle/123456789/6798
AB  - Nanocrystalline cobalt magnesium ferrites with varying cobalt and magnesium content (CoxMg1-xFe2O4, 0<x<1) were synthesized using the sol-gel self-combustion method with citric acid as fuel, followed by calcination at 700 °C for 2 hours. Structural characterization was performed using Xray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and Raman spectroscopy. It confirmed the formation of agglomerated nanocrystalline ferrites with an inverse cubic spinel structure. The optical band gap energy was determined using UV/Vis spectrophotometry. It reduced with increased Co content. Visible light photocatalytic activity was tested using natural and artificial light sources through a series of experimental degradations of the methylene blue (MB) solution.
PB  - Belgrade : Materials Research Society of Serbia
C3  - Twenty-first Annual Conference YUCOMAT 2019 & Eleventh World Round Table Conference on Sintering WRTCS 2019, Herceg Novi, Montenegro, September 2-6, 2019, Programme and The Book of Abstracts
T1  - Structure, morphology and photocatalytic properties of CoxMg1-xFe2O4 (0<x<1) spinel ferrites obtained by sol-gel synthesis
EP  - 126
SP  - 126
UR  - https://hdl.handle.net/21.15107/rcub_machinery_6798
ER  - 
@conference{
author = "Vasiljević, Zorka Ž. and Dojčinović, Milena and Pavlović, Vera P. and Vujančević, Jelena and Tadić, Nenad and Nikolić, Maria Vesna",
year = "2019",
abstract = "Nanocrystalline cobalt magnesium ferrites with varying cobalt and magnesium content (CoxMg1-xFe2O4, 0<x<1) were synthesized using the sol-gel self-combustion method with citric acid as fuel, followed by calcination at 700 °C for 2 hours. Structural characterization was performed using Xray diffraction (XRD), field emission scanning electron microscopy (FE-SEM) and Raman spectroscopy. It confirmed the formation of agglomerated nanocrystalline ferrites with an inverse cubic spinel structure. The optical band gap energy was determined using UV/Vis spectrophotometry. It reduced with increased Co content. Visible light photocatalytic activity was tested using natural and artificial light sources through a series of experimental degradations of the methylene blue (MB) solution.",
publisher = "Belgrade : Materials Research Society of Serbia",
journal = "Twenty-first Annual Conference YUCOMAT 2019 & Eleventh World Round Table Conference on Sintering WRTCS 2019, Herceg Novi, Montenegro, September 2-6, 2019, Programme and The Book of Abstracts",
title = "Structure, morphology and photocatalytic properties of CoxMg1-xFe2O4 (0<x<1) spinel ferrites obtained by sol-gel synthesis",
pages = "126-126",
url = "https://hdl.handle.net/21.15107/rcub_machinery_6798"
}
Vasiljević, Z. Ž., Dojčinović, M., Pavlović, V. P., Vujančević, J., Tadić, N.,& Nikolić, M. V.. (2019). Structure, morphology and photocatalytic properties of CoxMg1-xFe2O4 (0<x<1) spinel ferrites obtained by sol-gel synthesis. in Twenty-first Annual Conference YUCOMAT 2019 & Eleventh World Round Table Conference on Sintering WRTCS 2019, Herceg Novi, Montenegro, September 2-6, 2019, Programme and The Book of Abstracts
Belgrade : Materials Research Society of Serbia., 126-126.
https://hdl.handle.net/21.15107/rcub_machinery_6798
Vasiljević ZŽ, Dojčinović M, Pavlović VP, Vujančević J, Tadić N, Nikolić MV. Structure, morphology and photocatalytic properties of CoxMg1-xFe2O4 (0<x<1) spinel ferrites obtained by sol-gel synthesis. in Twenty-first Annual Conference YUCOMAT 2019 & Eleventh World Round Table Conference on Sintering WRTCS 2019, Herceg Novi, Montenegro, September 2-6, 2019, Programme and The Book of Abstracts. 2019;:126-126.
https://hdl.handle.net/21.15107/rcub_machinery_6798 .
Vasiljević, Zorka Ž., Dojčinović, Milena, Pavlović, Vera P., Vujančević, Jelena, Tadić, Nenad, Nikolić, Maria Vesna, "Structure, morphology and photocatalytic properties of CoxMg1-xFe2O4 (0<x<1) spinel ferrites obtained by sol-gel synthesis" in Twenty-first Annual Conference YUCOMAT 2019 & Eleventh World Round Table Conference on Sintering WRTCS 2019, Herceg Novi, Montenegro, September 2-6, 2019, Programme and The Book of Abstracts (2019):126-126,
https://hdl.handle.net/21.15107/rcub_machinery_6798 .

Influence of Co2+ ions on photocatalytic properties of MgFe2O4 ferrites

Vasiljević, Zorka Ž.; Dojčinović, Milena; Pavlović, Vera P.; Vujančević, Jelena; Marković, Smilja; Tadić, Nenad; Nikolić, Maria Vesna

(Institute for Multidisciplinary Research, University of Belgrade, 2019)

TY  - CONF
AU  - Vasiljević, Zorka Ž.
AU  - Dojčinović, Milena
AU  - Pavlović, Vera P.
AU  - Vujančević, Jelena
AU  - Marković, Smilja
AU  - Tadić, Nenad
AU  - Nikolić, Maria Vesna
PY  - 2019
UR  - https://machinery.mas.bg.ac.rs/handle/123456789/6797
AB  - In this work, spinel magnesium cobalt ferrites (CoxMg1-xFe2O4, x = 0.0, 0.1, 0.3, 0.5, 0.7, 0.9) were synthesized by a sol-gel combustion method. Magnesium nitrate, cobalt nitrate and iron nitrate were used as oxidizers and citric acid was used as a reducing agent. The effects of cobalt ions on structural and morphological properties were investigated and characterized by X-ray diffraction (XRD), Raman spectroscopy, Field emission scanning electron microscope (FESEM) and Fourier transform infrared (FT-IR) spectroscopy. A cubic spinel structure formed with a varied distribution of cobalt and magnesium ions on tetrahedral and octahedral sites that depended on their content. All ferrite powders consisted of multigrain agglomerates. Optical properties were investigated by UV- vis spectrophotometry. The photocatalytic activity of as prepared samples was evaluated by measuring the rate of photodegradation reaction of methylene blue (MB) under visible light irradiation. After 240 min, compared to other samples, the sample labeled as Co0.1Mg0.9Fe2O4 showed the best rate of photodecomposition of MB resulting in reduction of 90% of its initial concentration.
PB  - Institute for Multidisciplinary Research, University of Belgrade
C3  - 5th Conference of The Serbian Society for Ceramic Materials - 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia, Programme and the Book of Abstracts
T1  - Influence of Co2+ ions on photocatalytic properties of MgFe2O4 ferrites
EP  - 73
SP  - 73
UR  - https://hdl.handle.net/21.15107/rcub_machinery_6797
ER  - 
@conference{
author = "Vasiljević, Zorka Ž. and Dojčinović, Milena and Pavlović, Vera P. and Vujančević, Jelena and Marković, Smilja and Tadić, Nenad and Nikolić, Maria Vesna",
year = "2019",
abstract = "In this work, spinel magnesium cobalt ferrites (CoxMg1-xFe2O4, x = 0.0, 0.1, 0.3, 0.5, 0.7, 0.9) were synthesized by a sol-gel combustion method. Magnesium nitrate, cobalt nitrate and iron nitrate were used as oxidizers and citric acid was used as a reducing agent. The effects of cobalt ions on structural and morphological properties were investigated and characterized by X-ray diffraction (XRD), Raman spectroscopy, Field emission scanning electron microscope (FESEM) and Fourier transform infrared (FT-IR) spectroscopy. A cubic spinel structure formed with a varied distribution of cobalt and magnesium ions on tetrahedral and octahedral sites that depended on their content. All ferrite powders consisted of multigrain agglomerates. Optical properties were investigated by UV- vis spectrophotometry. The photocatalytic activity of as prepared samples was evaluated by measuring the rate of photodegradation reaction of methylene blue (MB) under visible light irradiation. After 240 min, compared to other samples, the sample labeled as Co0.1Mg0.9Fe2O4 showed the best rate of photodecomposition of MB resulting in reduction of 90% of its initial concentration.",
publisher = "Institute for Multidisciplinary Research, University of Belgrade",
journal = "5th Conference of The Serbian Society for Ceramic Materials - 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia, Programme and the Book of Abstracts",
title = "Influence of Co2+ ions on photocatalytic properties of MgFe2O4 ferrites",
pages = "73-73",
url = "https://hdl.handle.net/21.15107/rcub_machinery_6797"
}
Vasiljević, Z. Ž., Dojčinović, M., Pavlović, V. P., Vujančević, J., Marković, S., Tadić, N.,& Nikolić, M. V.. (2019). Influence of Co2+ ions on photocatalytic properties of MgFe2O4 ferrites. in 5th Conference of The Serbian Society for Ceramic Materials - 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia, Programme and the Book of Abstracts
Institute for Multidisciplinary Research, University of Belgrade., 73-73.
https://hdl.handle.net/21.15107/rcub_machinery_6797
Vasiljević ZŽ, Dojčinović M, Pavlović VP, Vujančević J, Marković S, Tadić N, Nikolić MV. Influence of Co2+ ions on photocatalytic properties of MgFe2O4 ferrites. in 5th Conference of The Serbian Society for Ceramic Materials - 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia, Programme and the Book of Abstracts. 2019;:73-73.
https://hdl.handle.net/21.15107/rcub_machinery_6797 .
Vasiljević, Zorka Ž., Dojčinović, Milena, Pavlović, Vera P., Vujančević, Jelena, Marković, Smilja, Tadić, Nenad, Nikolić, Maria Vesna, "Influence of Co2+ ions on photocatalytic properties of MgFe2O4 ferrites" in 5th Conference of The Serbian Society for Ceramic Materials - 5CSCS-2019, June 11-13, 2019, Belgrade, Serbia, Programme and the Book of Abstracts (2019):73-73,
https://hdl.handle.net/21.15107/rcub_machinery_6797 .

Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing

Nikolić, Maria Vesna; Vasiljević, Zorka Ž.; Luković, Miloljub D.; Pavlović, Vera P.; Krstić, Jugoslav B.; Vujančević, Jelena; Tadić, Nenad; Vlahović, Branislav; Pavlović, Vladimir B.

(Wiley, 2019)

TY  - JOUR
AU  - Nikolić, Maria Vesna
AU  - Vasiljević, Zorka Ž.
AU  - Luković, Miloljub D.
AU  - Pavlović, Vera P.
AU  - Krstić, Jugoslav B.
AU  - Vujančević, Jelena
AU  - Tadić, Nenad
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://machinery.mas.bg.ac.rs/handle/123456789/4066
AB  - Zinc ferrite nanocrystalline powder was obtained by solid state synthesis of starting zinc oxide and hematite nanopowders. Field emission scanning electron microscopy (FESEM) and transmission electron microscopy (TEM), X‐ray diffraction (XRD), X‐ray photoelectron spectroscopy (XPS) and Raman spectroscopy confirmed the formation of nanocrystalline zinc‐ferrite powder with a mixed spinel structure with small amounts of remaining zinc oxide and hematite as impurities. Thick film paste was formed and screen printed on test interdigitated PdAg electrodes on alumina substrate. Formation of a porous nanocrystalline structure was confirmed by scanning electron microscopy (SEM) and Hg porosimetry. Humidity sensing properties of zinc ferrite thick films were investigated by monitoring the change in impedance in the relative humidity interval 30‐90% in the frequency range 42 Hz – 1 MHz at room temperature (25 °C) and 50 °C. At 42 Hz at both analyzed temperatures the impedance reduced ~ 46 times in the humidity range 30‐90%. The dominant influence of grain boundaries was confirmed by analysis of complex impedance with an equivalent circuit.
PB  - Wiley
T2  - International Journal of Applied Ceramic Technology
T1  - Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing
EP  - 993
IS  - 3
SP  - 981
VL  - 16
DO  - 10.1111/ijac.13190
ER  - 
@article{
author = "Nikolić, Maria Vesna and Vasiljević, Zorka Ž. and Luković, Miloljub D. and Pavlović, Vera P. and Krstić, Jugoslav B. and Vujančević, Jelena and Tadić, Nenad and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2019",
abstract = "Zinc ferrite nanocrystalline powder was obtained by solid state synthesis of starting zinc oxide and hematite nanopowders. Field emission scanning electron microscopy (FESEM) and transmission electron microscopy (TEM), X‐ray diffraction (XRD), X‐ray photoelectron spectroscopy (XPS) and Raman spectroscopy confirmed the formation of nanocrystalline zinc‐ferrite powder with a mixed spinel structure with small amounts of remaining zinc oxide and hematite as impurities. Thick film paste was formed and screen printed on test interdigitated PdAg electrodes on alumina substrate. Formation of a porous nanocrystalline structure was confirmed by scanning electron microscopy (SEM) and Hg porosimetry. Humidity sensing properties of zinc ferrite thick films were investigated by monitoring the change in impedance in the relative humidity interval 30‐90% in the frequency range 42 Hz – 1 MHz at room temperature (25 °C) and 50 °C. At 42 Hz at both analyzed temperatures the impedance reduced ~ 46 times in the humidity range 30‐90%. The dominant influence of grain boundaries was confirmed by analysis of complex impedance with an equivalent circuit.",
publisher = "Wiley",
journal = "International Journal of Applied Ceramic Technology",
title = "Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing",
pages = "993-981",
number = "3",
volume = "16",
doi = "10.1111/ijac.13190"
}
Nikolić, M. V., Vasiljević, Z. Ž., Luković, M. D., Pavlović, V. P., Krstić, J. B., Vujančević, J., Tadić, N., Vlahović, B.,& Pavlović, V. B.. (2019). Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing. in International Journal of Applied Ceramic Technology
Wiley., 16(3), 981-993.
https://doi.org/10.1111/ijac.13190
Nikolić MV, Vasiljević ZŽ, Luković MD, Pavlović VP, Krstić JB, Vujančević J, Tadić N, Vlahović B, Pavlović VB. Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing. in International Journal of Applied Ceramic Technology. 2019;16(3):981-993.
doi:10.1111/ijac.13190 .
Nikolić, Maria Vesna, Vasiljević, Zorka Ž., Luković, Miloljub D., Pavlović, Vera P., Krstić, Jugoslav B., Vujančević, Jelena, Tadić, Nenad, Vlahović, Branislav, Pavlović, Vladimir B., "Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing" in International Journal of Applied Ceramic Technology, 16, no. 3 (2019):981-993,
https://doi.org/10.1111/ijac.13190 . .
37
15
38

Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing

Nikolić, Maria Vesna; Vasiljević, Zorka Ž.; Luković, Miloljub D.; Pavlović, Vera P.; Krstić, Jugoslav B.; Vujančević, Jelena; Tadić, Nenad; Vlahović, Branislav; Pavlović, Vladimir B.

(Wiley, Hoboken, 2019)

TY  - JOUR
AU  - Nikolić, Maria Vesna
AU  - Vasiljević, Zorka Ž.
AU  - Luković, Miloljub D.
AU  - Pavlović, Vera P.
AU  - Krstić, Jugoslav B.
AU  - Vujančević, Jelena
AU  - Tadić, Nenad
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://machinery.mas.bg.ac.rs/handle/123456789/3101
AB  - Zinc ferrite nanocrystalline powder was obtained by solid state synthesis of starting zinc oxide and hematite nanopowders. Field emission scanning electron microscopy and transmission electron microscopy, X-ray diffraction, X-ray photoelectron spectroscopy and Raman spectroscopy confirmed the formation of nanocrystalline zinc-ferrite powder with a mixed spinel structure with small amounts of remaining zinc oxide and hematite as impurities. Thick film paste was formed and screen printed on test interdigitated PdAg electrodes on alumina substrate. Formation of a porous nanocrystalline structure was confirmed by scanning electron microscopy and Hg porosimetry. Humidity sensing properties of zinc ferrite thick films were investigated by monitoring the change in impedance in the relative humidity interval 30%-90% in the frequency range 42 Hz-1 MHz at room temperature (25 degrees C) and 50 degrees C. At 42 Hz at both analyzed temperatures the impedance reduced 46 times in the humidity range 30%-90%. The dominant influence of grain boundaries was confirmed by analysis of complex impedance with an equivalent circuit.
PB  - Wiley, Hoboken
T2  - International Journal of Applied Ceramic Technology
T1  - Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing
EP  - 993
IS  - 3
SP  - 981
VL  - 16
DO  - 10.1111/ijac.13190
ER  - 
@article{
author = "Nikolić, Maria Vesna and Vasiljević, Zorka Ž. and Luković, Miloljub D. and Pavlović, Vera P. and Krstić, Jugoslav B. and Vujančević, Jelena and Tadić, Nenad and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2019",
abstract = "Zinc ferrite nanocrystalline powder was obtained by solid state synthesis of starting zinc oxide and hematite nanopowders. Field emission scanning electron microscopy and transmission electron microscopy, X-ray diffraction, X-ray photoelectron spectroscopy and Raman spectroscopy confirmed the formation of nanocrystalline zinc-ferrite powder with a mixed spinel structure with small amounts of remaining zinc oxide and hematite as impurities. Thick film paste was formed and screen printed on test interdigitated PdAg electrodes on alumina substrate. Formation of a porous nanocrystalline structure was confirmed by scanning electron microscopy and Hg porosimetry. Humidity sensing properties of zinc ferrite thick films were investigated by monitoring the change in impedance in the relative humidity interval 30%-90% in the frequency range 42 Hz-1 MHz at room temperature (25 degrees C) and 50 degrees C. At 42 Hz at both analyzed temperatures the impedance reduced 46 times in the humidity range 30%-90%. The dominant influence of grain boundaries was confirmed by analysis of complex impedance with an equivalent circuit.",
publisher = "Wiley, Hoboken",
journal = "International Journal of Applied Ceramic Technology",
title = "Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing",
pages = "993-981",
number = "3",
volume = "16",
doi = "10.1111/ijac.13190"
}
Nikolić, M. V., Vasiljević, Z. Ž., Luković, M. D., Pavlović, V. P., Krstić, J. B., Vujančević, J., Tadić, N., Vlahović, B.,& Pavlović, V. B.. (2019). Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing. in International Journal of Applied Ceramic Technology
Wiley, Hoboken., 16(3), 981-993.
https://doi.org/10.1111/ijac.13190
Nikolić MV, Vasiljević ZŽ, Luković MD, Pavlović VP, Krstić JB, Vujančević J, Tadić N, Vlahović B, Pavlović VB. Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing. in International Journal of Applied Ceramic Technology. 2019;16(3):981-993.
doi:10.1111/ijac.13190 .
Nikolić, Maria Vesna, Vasiljević, Zorka Ž., Luković, Miloljub D., Pavlović, Vera P., Krstić, Jugoslav B., Vujančević, Jelena, Tadić, Nenad, Vlahović, Branislav, Pavlović, Vladimir B., "Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing" in International Journal of Applied Ceramic Technology, 16, no. 3 (2019):981-993,
https://doi.org/10.1111/ijac.13190 . .
38
15
37

Finding optimal conditions and investigating the structure & morphology of cobalt/magnesium ferrite based cubic spinels (CoxMg1-xFe2O4) as photocatalysts

Dojčinović, Milena; Vasiljević, Zorka Ž.; Tadić, Nenad; Pavlović, Vera P.; Barišić, Dario; Pajić, Damir; Nikolić, Maria Vesna

(Belgrade : Institute of Technical Sciences of SASA, 2019)

TY  - CONF
AU  - Dojčinović, Milena
AU  - Vasiljević, Zorka Ž.
AU  - Tadić, Nenad
AU  - Pavlović, Vera P.
AU  - Barišić, Dario
AU  - Pajić, Damir
AU  - Nikolić, Maria Vesna
PY  - 2019
UR  - https://machinery.mas.bg.ac.rs/handle/123456789/6799
AB  - Cobalt/magnesium ferrites with various mole percentage ratio of the metals (obtained structures are CoxMg1-xFe2O4 with x being 0, 0.1, 0.3, 0.5, 0.7, 0.9, 1.0) were synthesized by sol-gel combustion synthesis using glycine as fuel, following the rules of propellant chemistry. The powders were then sintered at 700 °C for 3 hours. Obtained powders were characterized by X-Ray diffraction (XRD), scanning electron microscopy (SEM), Raman spectroscopy, UV/vis diffuse reflectance spectroscopy (DRS). Investigation of the magnetic properties was also conducted by vibrating sample magnetometry (VSM). The obtained powders were proved to be phase-pure cubic spinels which formed agglomerated micrograins. Series of photocatalytic experiments of methylene blue degradation were done. The influence of different experimental conditions was investigated including variations of: pH values, concentrations of the pollutant, masses of the photocatalyst, different light sources and therefore different light irradiation. Interesting results, including enhancement of the degradation rate with the introduction of cobalt into MgFe2O4 and decrease of the degradation rate with further increase of cobalt content and formation of hard agglomerates, open new possibilities for further investigation of the utilisation of Co/Mg ferrites as photocatalysts.
PB  - Belgrade : Institute of Technical Sciences of SASA
C3  - Program and the Book of Abstracts / Eighteenth Young Researchers' Conference - Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia
T1  - Finding optimal conditions and investigating the structure & morphology of cobalt/magnesium ferrite based cubic spinels (CoxMg1-xFe2O4) as photocatalysts
EP  - 71
SP  - 71
UR  - https://hdl.handle.net/21.15107/rcub_machinery_6799
ER  - 
@conference{
author = "Dojčinović, Milena and Vasiljević, Zorka Ž. and Tadić, Nenad and Pavlović, Vera P. and Barišić, Dario and Pajić, Damir and Nikolić, Maria Vesna",
year = "2019",
abstract = "Cobalt/magnesium ferrites with various mole percentage ratio of the metals (obtained structures are CoxMg1-xFe2O4 with x being 0, 0.1, 0.3, 0.5, 0.7, 0.9, 1.0) were synthesized by sol-gel combustion synthesis using glycine as fuel, following the rules of propellant chemistry. The powders were then sintered at 700 °C for 3 hours. Obtained powders were characterized by X-Ray diffraction (XRD), scanning electron microscopy (SEM), Raman spectroscopy, UV/vis diffuse reflectance spectroscopy (DRS). Investigation of the magnetic properties was also conducted by vibrating sample magnetometry (VSM). The obtained powders were proved to be phase-pure cubic spinels which formed agglomerated micrograins. Series of photocatalytic experiments of methylene blue degradation were done. The influence of different experimental conditions was investigated including variations of: pH values, concentrations of the pollutant, masses of the photocatalyst, different light sources and therefore different light irradiation. Interesting results, including enhancement of the degradation rate with the introduction of cobalt into MgFe2O4 and decrease of the degradation rate with further increase of cobalt content and formation of hard agglomerates, open new possibilities for further investigation of the utilisation of Co/Mg ferrites as photocatalysts.",
publisher = "Belgrade : Institute of Technical Sciences of SASA",
journal = "Program and the Book of Abstracts / Eighteenth Young Researchers' Conference - Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia",
title = "Finding optimal conditions and investigating the structure & morphology of cobalt/magnesium ferrite based cubic spinels (CoxMg1-xFe2O4) as photocatalysts",
pages = "71-71",
url = "https://hdl.handle.net/21.15107/rcub_machinery_6799"
}
Dojčinović, M., Vasiljević, Z. Ž., Tadić, N., Pavlović, V. P., Barišić, D., Pajić, D.,& Nikolić, M. V.. (2019). Finding optimal conditions and investigating the structure & morphology of cobalt/magnesium ferrite based cubic spinels (CoxMg1-xFe2O4) as photocatalysts. in Program and the Book of Abstracts / Eighteenth Young Researchers' Conference - Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia
Belgrade : Institute of Technical Sciences of SASA., 71-71.
https://hdl.handle.net/21.15107/rcub_machinery_6799
Dojčinović M, Vasiljević ZŽ, Tadić N, Pavlović VP, Barišić D, Pajić D, Nikolić MV. Finding optimal conditions and investigating the structure & morphology of cobalt/magnesium ferrite based cubic spinels (CoxMg1-xFe2O4) as photocatalysts. in Program and the Book of Abstracts / Eighteenth Young Researchers' Conference - Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia. 2019;:71-71.
https://hdl.handle.net/21.15107/rcub_machinery_6799 .
Dojčinović, Milena, Vasiljević, Zorka Ž., Tadić, Nenad, Pavlović, Vera P., Barišić, Dario, Pajić, Damir, Nikolić, Maria Vesna, "Finding optimal conditions and investigating the structure & morphology of cobalt/magnesium ferrite based cubic spinels (CoxMg1-xFe2O4) as photocatalysts" in Program and the Book of Abstracts / Eighteenth Young Researchers' Conference - Materials Sciences and Engineering, December 4-6, 2019, Belgrade, Serbia (2019):71-71,
https://hdl.handle.net/21.15107/rcub_machinery_6799 .

The effect of mechanical activation on synthesis and properties of MgAl2O4 ceramics

Obradović, Nina; Fahrenholtz, William G.; Filipović, Suzana; Kosanović, Darko; Dapčević, Aleksandra; Đorđević, Antonije; Balać, Igor; Pavlović, Vladimir B.

(Elsevier Sci Ltd, Oxford, 2019)

TY  - JOUR
AU  - Obradović, Nina
AU  - Fahrenholtz, William G.
AU  - Filipović, Suzana
AU  - Kosanović, Darko
AU  - Dapčević, Aleksandra
AU  - Đorđević, Antonije
AU  - Balać, Igor
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://machinery.mas.bg.ac.rs/handle/123456789/3133
AB  - Magnesium aluminate, MgAl2O4 and other alumina-based spinels are ceramics with high hardness, high melting point and mechanical strenght. Spinels can also be used as dielectrics in microwave applications. The goal of this study was to examine the effects of mechanical activation and sintering temperatures on physico-chemical properties of spinel. MgAl2O4 was produced by solid state reaction between MgO and alpha-Al2O3. The starting powders were mixed by ball milling to homogenize without significant particle size reduction. Mechanical activation of mixed powders was performed in a high-energy planetary ball mill in air for 1 h. Powders were compacted at 300 MPa. Heat treatments were performed in air, at temperatures ranging from 1200 to 1600 degrees C with 2 h dwell time, to determine the amount of spinel formation as a function of temperature. Phase composition and microstructure of initial powders and heated samples were determined by means of X-ray diffraction, particle size analysis, and scanning electron microscopy. The influences of milling and consolidation parameters were studied by electrical measurements and mechanical characterization. The main conclusion of this study was that mechanical activation for 60 min initiated a mechano-chemical reaction, resulted in spinel formation at much lower temperatures than within non-activated powders, and indicated that final sintering stage started at much lower temperatures for activated powders. Changes in microstructure parameters, as a consequence of mechanical treatment and subsequent heating of investigated powder mixtures, strongly affect electrical and mechanical properties of the final ceramics.
PB  - Elsevier Sci Ltd, Oxford
T2  - Ceramics International
T1  - The effect of mechanical activation on synthesis and properties of MgAl2O4 ceramics
EP  - 12021
IS  - 9
SP  - 12015
VL  - 45
DO  - 10.1016/j.ceramint.2019.03.095
ER  - 
@article{
author = "Obradović, Nina and Fahrenholtz, William G. and Filipović, Suzana and Kosanović, Darko and Dapčević, Aleksandra and Đorđević, Antonije and Balać, Igor and Pavlović, Vladimir B.",
year = "2019",
abstract = "Magnesium aluminate, MgAl2O4 and other alumina-based spinels are ceramics with high hardness, high melting point and mechanical strenght. Spinels can also be used as dielectrics in microwave applications. The goal of this study was to examine the effects of mechanical activation and sintering temperatures on physico-chemical properties of spinel. MgAl2O4 was produced by solid state reaction between MgO and alpha-Al2O3. The starting powders were mixed by ball milling to homogenize without significant particle size reduction. Mechanical activation of mixed powders was performed in a high-energy planetary ball mill in air for 1 h. Powders were compacted at 300 MPa. Heat treatments were performed in air, at temperatures ranging from 1200 to 1600 degrees C with 2 h dwell time, to determine the amount of spinel formation as a function of temperature. Phase composition and microstructure of initial powders and heated samples were determined by means of X-ray diffraction, particle size analysis, and scanning electron microscopy. The influences of milling and consolidation parameters were studied by electrical measurements and mechanical characterization. The main conclusion of this study was that mechanical activation for 60 min initiated a mechano-chemical reaction, resulted in spinel formation at much lower temperatures than within non-activated powders, and indicated that final sintering stage started at much lower temperatures for activated powders. Changes in microstructure parameters, as a consequence of mechanical treatment and subsequent heating of investigated powder mixtures, strongly affect electrical and mechanical properties of the final ceramics.",
publisher = "Elsevier Sci Ltd, Oxford",
journal = "Ceramics International",
title = "The effect of mechanical activation on synthesis and properties of MgAl2O4 ceramics",
pages = "12021-12015",
number = "9",
volume = "45",
doi = "10.1016/j.ceramint.2019.03.095"
}
Obradović, N., Fahrenholtz, W. G., Filipović, S., Kosanović, D., Dapčević, A., Đorđević, A., Balać, I.,& Pavlović, V. B.. (2019). The effect of mechanical activation on synthesis and properties of MgAl2O4 ceramics. in Ceramics International
Elsevier Sci Ltd, Oxford., 45(9), 12015-12021.
https://doi.org/10.1016/j.ceramint.2019.03.095
Obradović N, Fahrenholtz WG, Filipović S, Kosanović D, Dapčević A, Đorđević A, Balać I, Pavlović VB. The effect of mechanical activation on synthesis and properties of MgAl2O4 ceramics. in Ceramics International. 2019;45(9):12015-12021.
doi:10.1016/j.ceramint.2019.03.095 .
Obradović, Nina, Fahrenholtz, William G., Filipović, Suzana, Kosanović, Darko, Dapčević, Aleksandra, Đorđević, Antonije, Balać, Igor, Pavlović, Vladimir B., "The effect of mechanical activation on synthesis and properties of MgAl2O4 ceramics" in Ceramics International, 45, no. 9 (2019):12015-12021,
https://doi.org/10.1016/j.ceramint.2019.03.095 . .
27
12
26

Characterization of MgAl2O4 Sintered Ceramics

Obradović, Nina; Fahrenholtz, William G.; Filipović, Suzana; Corlett, Cole; Đorđević, Pavle; Rogan, Jelena; Vulić, Predrag J.; Buljak, Vladimir; Pavlović, Vladimir B.

(Međunarodni Institut za nauku o sinterovanju, Beograd, 2019)

TY  - JOUR
AU  - Obradović, Nina
AU  - Fahrenholtz, William G.
AU  - Filipović, Suzana
AU  - Corlett, Cole
AU  - Đorđević, Pavle
AU  - Rogan, Jelena
AU  - Vulić, Predrag J.
AU  - Buljak, Vladimir
AU  - Pavlović, Vladimir B.
PY  - 2019
UR  - https://machinery.mas.bg.ac.rs/handle/123456789/3235
AB  - Single phase MgAl2O4 was made from a one-to-one molar ratio of MgO and Al2O3 powders mixed using ball-milling. Mixtures of MgO and Al2O3 were subsequently treated in planetary ball mill for 30, 60, 90 and 120 minutes in air. The aim of this study was to examine phase composition, microstructure, and densification behavior of sintered specimens. After sintering in dilatometer at 1500 degrees C, the powder was converted to single phase MgAl2O4. The results show that mechanical activation improved the densification behavior of MgAl2O4 sintered specimens, and it reduced the onset temperature for sintering by approx. 100 degrees C. Based on dilatometer data, powders were subsequently densified at 1450 degrees C by hot pressing. Almost all specimens exhibited full density, while sample activated for 30 minutes showed the fastest densification rate.
PB  - Međunarodni Institut za nauku o sinterovanju, Beograd
T2  - Science of Sintering
T1  - Characterization of MgAl2O4 Sintered Ceramics
EP  - 376
IS  - 4
SP  - 363
VL  - 51
DO  - 10.2298/SOS1904363O
ER  - 
@article{
author = "Obradović, Nina and Fahrenholtz, William G. and Filipović, Suzana and Corlett, Cole and Đorđević, Pavle and Rogan, Jelena and Vulić, Predrag J. and Buljak, Vladimir and Pavlović, Vladimir B.",
year = "2019",
abstract = "Single phase MgAl2O4 was made from a one-to-one molar ratio of MgO and Al2O3 powders mixed using ball-milling. Mixtures of MgO and Al2O3 were subsequently treated in planetary ball mill for 30, 60, 90 and 120 minutes in air. The aim of this study was to examine phase composition, microstructure, and densification behavior of sintered specimens. After sintering in dilatometer at 1500 degrees C, the powder was converted to single phase MgAl2O4. The results show that mechanical activation improved the densification behavior of MgAl2O4 sintered specimens, and it reduced the onset temperature for sintering by approx. 100 degrees C. Based on dilatometer data, powders were subsequently densified at 1450 degrees C by hot pressing. Almost all specimens exhibited full density, while sample activated for 30 minutes showed the fastest densification rate.",
publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd",
journal = "Science of Sintering",
title = "Characterization of MgAl2O4 Sintered Ceramics",
pages = "376-363",
number = "4",
volume = "51",
doi = "10.2298/SOS1904363O"
}
Obradović, N., Fahrenholtz, W. G., Filipović, S., Corlett, C., Đorđević, P., Rogan, J., Vulić, P. J., Buljak, V.,& Pavlović, V. B.. (2019). Characterization of MgAl2O4 Sintered Ceramics. in Science of Sintering
Međunarodni Institut za nauku o sinterovanju, Beograd., 51(4), 363-376.
https://doi.org/10.2298/SOS1904363O
Obradović N, Fahrenholtz WG, Filipović S, Corlett C, Đorđević P, Rogan J, Vulić PJ, Buljak V, Pavlović VB. Characterization of MgAl2O4 Sintered Ceramics. in Science of Sintering. 2019;51(4):363-376.
doi:10.2298/SOS1904363O .
Obradović, Nina, Fahrenholtz, William G., Filipović, Suzana, Corlett, Cole, Đorđević, Pavle, Rogan, Jelena, Vulić, Predrag J., Buljak, Vladimir, Pavlović, Vladimir B., "Characterization of MgAl2O4 Sintered Ceramics" in Science of Sintering, 51, no. 4 (2019):363-376,
https://doi.org/10.2298/SOS1904363O . .
15
7
16

Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films

Nikolić, Maria Vesna; Vasiljević, Zorka Ž.; Luković, Miloljub D.; Pavlović, Vera P.; Vujančević, Jelena; Radovanović, Milan; Krstić, Jugoslav B.; Vlahović, Branislav; Pavlović, Vladimir B.

(Elsevier Science Sa, Lausanne, 2018)

TY  - JOUR
AU  - Nikolić, Maria Vesna
AU  - Vasiljević, Zorka Ž.
AU  - Luković, Miloljub D.
AU  - Pavlović, Vera P.
AU  - Vujančević, Jelena
AU  - Radovanović, Milan
AU  - Krstić, Jugoslav B.
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2018
UR  - https://machinery.mas.bg.ac.rs/handle/123456789/3945
AB  - Pseudobrookite based nanopowder was obtained by solid state synthesis of starting hematite and anatase nanopowders in the weight ratio 55:45. Structural and morphological properties were analyzed using X-ray diffraction (XRD), BET, X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, UV/Vis diffuse reflectance spectroscopy, Field emission scanning electron microscopy (FESEM) and Transmission electron microscopy (TEM) confirming the formation of nanocrystalline pseudobrookite. The obtained powder was mixed with a binder (ethyl cellulose), dispersant (alpha-terpinol) and adhesion agents (acetic acid and distilled water) to obtain a thick film paste. It was screen printed on alumina substrate with interdigitated PdAg electrodes and fired at 600 degrees C for 30 min. Formation of a porous nanocrystalline thick film structure was shown using Scanning electron microscopy (SEM), while Hall measurements enabled determination of carrier mobility. Change of impedance response in the frequency range 42 Hz-1 MHz with humidity was analyzed at room temperature (25 degrees C) and 50 degrees C in the relative humidity range 30-90% and 40-90%, respectively. At 42 Hz, and room temperature the impedance reduced similar to 28 times, while at 50 degrees C it reduced similar to 147 times in the relative humidity range 40-90%. The sensor showed rapid response (16 s) and relatively low hysteresis (8.39% at 25 degrees C and 2.64% at 50 degrees C) showing that this is a promising material for application in humidity sensing.
PB  - Elsevier Science Sa, Lausanne
T2  - Sensors and Actuators B-Chemical
T1  - Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films
EP  - 664
SP  - 654
VL  - 277
DO  - 10.1016/j.snb.2018.09.063
ER  - 
@article{
author = "Nikolić, Maria Vesna and Vasiljević, Zorka Ž. and Luković, Miloljub D. and Pavlović, Vera P. and Vujančević, Jelena and Radovanović, Milan and Krstić, Jugoslav B. and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2018",
abstract = "Pseudobrookite based nanopowder was obtained by solid state synthesis of starting hematite and anatase nanopowders in the weight ratio 55:45. Structural and morphological properties were analyzed using X-ray diffraction (XRD), BET, X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, UV/Vis diffuse reflectance spectroscopy, Field emission scanning electron microscopy (FESEM) and Transmission electron microscopy (TEM) confirming the formation of nanocrystalline pseudobrookite. The obtained powder was mixed with a binder (ethyl cellulose), dispersant (alpha-terpinol) and adhesion agents (acetic acid and distilled water) to obtain a thick film paste. It was screen printed on alumina substrate with interdigitated PdAg electrodes and fired at 600 degrees C for 30 min. Formation of a porous nanocrystalline thick film structure was shown using Scanning electron microscopy (SEM), while Hall measurements enabled determination of carrier mobility. Change of impedance response in the frequency range 42 Hz-1 MHz with humidity was analyzed at room temperature (25 degrees C) and 50 degrees C in the relative humidity range 30-90% and 40-90%, respectively. At 42 Hz, and room temperature the impedance reduced similar to 28 times, while at 50 degrees C it reduced similar to 147 times in the relative humidity range 40-90%. The sensor showed rapid response (16 s) and relatively low hysteresis (8.39% at 25 degrees C and 2.64% at 50 degrees C) showing that this is a promising material for application in humidity sensing.",
publisher = "Elsevier Science Sa, Lausanne",
journal = "Sensors and Actuators B-Chemical",
title = "Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films",
pages = "664-654",
volume = "277",
doi = "10.1016/j.snb.2018.09.063"
}
Nikolić, M. V., Vasiljević, Z. Ž., Luković, M. D., Pavlović, V. P., Vujančević, J., Radovanović, M., Krstić, J. B., Vlahović, B.,& Pavlović, V. B.. (2018). Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films. in Sensors and Actuators B-Chemical
Elsevier Science Sa, Lausanne., 277, 654-664.
https://doi.org/10.1016/j.snb.2018.09.063
Nikolić MV, Vasiljević ZŽ, Luković MD, Pavlović VP, Vujančević J, Radovanović M, Krstić JB, Vlahović B, Pavlović VB. Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films. in Sensors and Actuators B-Chemical. 2018;277:654-664.
doi:10.1016/j.snb.2018.09.063 .
Nikolić, Maria Vesna, Vasiljević, Zorka Ž., Luković, Miloljub D., Pavlović, Vera P., Vujančević, Jelena, Radovanović, Milan, Krstić, Jugoslav B., Vlahović, Branislav, Pavlović, Vladimir B., "Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films" in Sensors and Actuators B-Chemical, 277 (2018):654-664,
https://doi.org/10.1016/j.snb.2018.09.063 . .
40
22
38

Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films

Nikolić, Maria Vesna; Vasiljević, Zorka Ž.; Luković, Miloljub D.; Pavlović, Vera P.; Vujančević, Jelena; Radovanović, Milan; Krstić, Jugoslav B.; Vlahović, Branislav; Pavlović, Vladimir B.

(Elsevier Science Sa, Lausanne, 2018)

TY  - JOUR
AU  - Nikolić, Maria Vesna
AU  - Vasiljević, Zorka Ž.
AU  - Luković, Miloljub D.
AU  - Pavlović, Vera P.
AU  - Vujančević, Jelena
AU  - Radovanović, Milan
AU  - Krstić, Jugoslav B.
AU  - Vlahović, Branislav
AU  - Pavlović, Vladimir B.
PY  - 2018
UR  - https://machinery.mas.bg.ac.rs/handle/123456789/2887
AB  - Pseudobrookite based nanopowder was obtained by solid state synthesis of starting hematite and anatase nanopowders in the weight ratio 55:45. Structural and morphological properties were analyzed using X-ray diffraction (XRD), BET, X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, UV/Vis diffuse reflectance spectroscopy, Field emission scanning electron microscopy (FESEM) and Transmission electron microscopy (TEM) confirming the formation of nanocrystalline pseudobrookite. The obtained powder was mixed with a binder (ethyl cellulose), dispersant (alpha-terpinol) and adhesion agents (acetic acid and distilled water) to obtain a thick film paste. It was screen printed on alumina substrate with interdigitated PdAg electrodes and fired at 600 degrees C for 30 min. Formation of a porous nanocrystalline thick film structure was shown using Scanning electron microscopy (SEM), while Hall measurements enabled determination of carrier mobility. Change of impedance response in the frequency range 42 Hz-1 MHz with humidity was analyzed at room temperature (25 degrees C) and 50 degrees C in the relative humidity range 30-90% and 40-90%, respectively. At 42 Hz, and room temperature the impedance reduced similar to 28 times, while at 50 degrees C it reduced similar to 147 times in the relative humidity range 40-90%. The sensor showed rapid response (16 s) and relatively low hysteresis (8.39% at 25 degrees C and 2.64% at 50 degrees C) showing that this is a promising material for application in humidity sensing.
PB  - Elsevier Science Sa, Lausanne
T2  - Sensors and Actuators B-Chemical
T1  - Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films
EP  - 664
SP  - 654
VL  - 277
DO  - 10.1016/j.snb.2018.09.063
ER  - 
@article{
author = "Nikolić, Maria Vesna and Vasiljević, Zorka Ž. and Luković, Miloljub D. and Pavlović, Vera P. and Vujančević, Jelena and Radovanović, Milan and Krstić, Jugoslav B. and Vlahović, Branislav and Pavlović, Vladimir B.",
year = "2018",
abstract = "Pseudobrookite based nanopowder was obtained by solid state synthesis of starting hematite and anatase nanopowders in the weight ratio 55:45. Structural and morphological properties were analyzed using X-ray diffraction (XRD), BET, X-ray photoelectron spectroscopy (XPS), Raman spectroscopy, UV/Vis diffuse reflectance spectroscopy, Field emission scanning electron microscopy (FESEM) and Transmission electron microscopy (TEM) confirming the formation of nanocrystalline pseudobrookite. The obtained powder was mixed with a binder (ethyl cellulose), dispersant (alpha-terpinol) and adhesion agents (acetic acid and distilled water) to obtain a thick film paste. It was screen printed on alumina substrate with interdigitated PdAg electrodes and fired at 600 degrees C for 30 min. Formation of a porous nanocrystalline thick film structure was shown using Scanning electron microscopy (SEM), while Hall measurements enabled determination of carrier mobility. Change of impedance response in the frequency range 42 Hz-1 MHz with humidity was analyzed at room temperature (25 degrees C) and 50 degrees C in the relative humidity range 30-90% and 40-90%, respectively. At 42 Hz, and room temperature the impedance reduced similar to 28 times, while at 50 degrees C it reduced similar to 147 times in the relative humidity range 40-90%. The sensor showed rapid response (16 s) and relatively low hysteresis (8.39% at 25 degrees C and 2.64% at 50 degrees C) showing that this is a promising material for application in humidity sensing.",
publisher = "Elsevier Science Sa, Lausanne",
journal = "Sensors and Actuators B-Chemical",
title = "Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films",
pages = "664-654",
volume = "277",
doi = "10.1016/j.snb.2018.09.063"
}
Nikolić, M. V., Vasiljević, Z. Ž., Luković, M. D., Pavlović, V. P., Vujančević, J., Radovanović, M., Krstić, J. B., Vlahović, B.,& Pavlović, V. B.. (2018). Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films. in Sensors and Actuators B-Chemical
Elsevier Science Sa, Lausanne., 277, 654-664.
https://doi.org/10.1016/j.snb.2018.09.063
Nikolić MV, Vasiljević ZŽ, Luković MD, Pavlović VP, Vujančević J, Radovanović M, Krstić JB, Vlahović B, Pavlović VB. Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films. in Sensors and Actuators B-Chemical. 2018;277:654-664.
doi:10.1016/j.snb.2018.09.063 .
Nikolić, Maria Vesna, Vasiljević, Zorka Ž., Luković, Miloljub D., Pavlović, Vera P., Vujančević, Jelena, Radovanović, Milan, Krstić, Jugoslav B., Vlahović, Branislav, Pavlović, Vladimir B., "Humidity sensing properties of nanocrystalline pseudobrookite (Fe2TiO5) based thick films" in Sensors and Actuators B-Chemical, 277 (2018):654-664,
https://doi.org/10.1016/j.snb.2018.09.063 . .
40
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38

Physical Properties of Sintered Alumina Doped with Different Oxides

Filipović, Suzana; Obradović, Nina; Marković, Smilja; Đorđević, Antonije; Balać, Igor; Dapčević, Aleksandra; Rogan, Jelena; Pavlović, Vladimir B.

(Međunarodni Institut za nauku o sinterovanju, Beograd, 2018)

TY  - JOUR
AU  - Filipović, Suzana
AU  - Obradović, Nina
AU  - Marković, Smilja
AU  - Đorđević, Antonije
AU  - Balać, Igor
AU  - Dapčević, Aleksandra
AU  - Rogan, Jelena
AU  - Pavlović, Vladimir B.
PY  - 2018
UR  - https://machinery.mas.bg.ac.rs/handle/123456789/2844
AB  - Corundum (alpha-alumina) is a suiTab. material for usage in various industry fields owing to its chemical stability, electrical and mechanical features. It is known that properties of ceramics could be modified by addition of different oxides, as well as by changing the consolidation parameters. In this respect, alumina was doped with 1 wt.% of Cr2O3, Mn2O3 and NiO, followed by 1 hour of mechanical activation in a high-energy planetary ball mill. A sensitive dilatometer was used for sintering of powder mixtures up to 1400 degrees C and recording the obtained dilatation. The final density varied between cca. 1.9 and 3.3 g/cm(3). Microstructural changes were detected by SEM measurements. Changes in electrical permittivity and loss tangent were associated with the preparation conditions (types of additives, duration of mechanical activation). For a given mixture, the sintering increases the relative permittivity and decreases losses, exhibiting the optimal values of 8.32 and 0.027, respectively, for the sample activated 60 minutes and sintered, with the addition of MnO2. Mechanical measurements indicate significant differences in strength with the addition of different transition metal oxides. Samples with Mn and Ni, activated and sintered, with strength of 121 and 86 MPa, respectively, have a significantly higher tensile strength than the other tested samples, due to their more compact microstructures.
PB  - Međunarodni Institut za nauku o sinterovanju, Beograd
T2  - Science of Sintering
T1  - Physical Properties of Sintered Alumina Doped with Different Oxides
EP  - 419
IS  - 4
SP  - 409
VL  - 50
DO  - 10.2298/SOS1804409F
ER  - 
@article{
author = "Filipović, Suzana and Obradović, Nina and Marković, Smilja and Đorđević, Antonije and Balać, Igor and Dapčević, Aleksandra and Rogan, Jelena and Pavlović, Vladimir B.",
year = "2018",
abstract = "Corundum (alpha-alumina) is a suiTab. material for usage in various industry fields owing to its chemical stability, electrical and mechanical features. It is known that properties of ceramics could be modified by addition of different oxides, as well as by changing the consolidation parameters. In this respect, alumina was doped with 1 wt.% of Cr2O3, Mn2O3 and NiO, followed by 1 hour of mechanical activation in a high-energy planetary ball mill. A sensitive dilatometer was used for sintering of powder mixtures up to 1400 degrees C and recording the obtained dilatation. The final density varied between cca. 1.9 and 3.3 g/cm(3). Microstructural changes were detected by SEM measurements. Changes in electrical permittivity and loss tangent were associated with the preparation conditions (types of additives, duration of mechanical activation). For a given mixture, the sintering increases the relative permittivity and decreases losses, exhibiting the optimal values of 8.32 and 0.027, respectively, for the sample activated 60 minutes and sintered, with the addition of MnO2. Mechanical measurements indicate significant differences in strength with the addition of different transition metal oxides. Samples with Mn and Ni, activated and sintered, with strength of 121 and 86 MPa, respectively, have a significantly higher tensile strength than the other tested samples, due to their more compact microstructures.",
publisher = "Međunarodni Institut za nauku o sinterovanju, Beograd",
journal = "Science of Sintering",
title = "Physical Properties of Sintered Alumina Doped with Different Oxides",
pages = "419-409",
number = "4",
volume = "50",
doi = "10.2298/SOS1804409F"
}
Filipović, S., Obradović, N., Marković, S., Đorđević, A., Balać, I., Dapčević, A., Rogan, J.,& Pavlović, V. B.. (2018). Physical Properties of Sintered Alumina Doped with Different Oxides. in Science of Sintering
Međunarodni Institut za nauku o sinterovanju, Beograd., 50(4), 409-419.
https://doi.org/10.2298/SOS1804409F
Filipović S, Obradović N, Marković S, Đorđević A, Balać I, Dapčević A, Rogan J, Pavlović VB. Physical Properties of Sintered Alumina Doped with Different Oxides. in Science of Sintering. 2018;50(4):409-419.
doi:10.2298/SOS1804409F .
Filipović, Suzana, Obradović, Nina, Marković, Smilja, Đorđević, Antonije, Balać, Igor, Dapčević, Aleksandra, Rogan, Jelena, Pavlović, Vladimir B., "Physical Properties of Sintered Alumina Doped with Different Oxides" in Science of Sintering, 50, no. 4 (2018):409-419,
https://doi.org/10.2298/SOS1804409F . .
11
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17