Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing
2019
Authors
Nikolić, Maria VesnaVasiljević, Zorka Ž.
Luković, Miloljub D.
Pavlović, Vera P.
Krstić, Jugoslav B.
Vujančević, Jelena
Tadić, Nenad
Vlahović, Branislav
Pavlović, Vladimir B.
Article (Accepted Version)
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Show full item recordAbstract
Zinc ferrite nanocrystalline powder was obtained by solid state synthesis of starting zinc oxide and hematite nanopowders. Field emission scanning electron microscopy (FESEM) and transmission electron microscopy (TEM), X‐ray diffraction (XRD), X‐ray photoelectron spectroscopy (XPS) and Raman spectroscopy confirmed the formation of nanocrystalline zinc‐ferrite powder with a mixed spinel structure with small amounts of remaining zinc oxide and hematite as impurities. Thick film paste was formed and screen printed on test interdigitated PdAg electrodes on alumina substrate. Formation of a porous nanocrystalline structure was confirmed by scanning electron microscopy (SEM) and Hg porosimetry. Humidity sensing properties of zinc ferrite thick films were investigated by monitoring the change in impedance in the relative humidity interval 30‐90% in the frequency range 42 Hz – 1 MHz at room temperature (25 °C) and 50 °C. At 42 Hz at both analyzed temperatures the impedance reduced ~ 46 times i...n the humidity range 30‐90%. The dominant influence of grain boundaries was confirmed by analysis of complex impedance with an equivalent circuit.
Keywords:
electrical properties / humidity sensor / thick film / zinc ferriteSource:
International Journal of Applied Ceramic Technology, 2019, 16, 3, 981-993Publisher:
- Wiley
Funding / projects:
- Zero- to Three-Dimensional Nanostructures for Application in Electronics and Renewable Energy Sources: Synthesis, Characterization and Processing (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45007)
- Lithium-ion batteries and fuel cells - research and development (RS-MESTD-Integrated and Interdisciplinary Research (IIR or III)-45014)
- Directed synthesis, structure and properties of multifunctional materials (RS-MESTD-Basic Research (BR or ON)-172057)
Note:
- This is the peer-reviewed version of the article: Nikolic, M.V., Vasiljevic, Z.Z., Lukovic, M.D., Pavlovic, V.P., Krstic, J.B., Vujancevic, J., Tadic, N., Vlahovic, B., Pavlovic, V.B. (2019). Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen‐printed thick films for application in humidity sensing. International Journal of Applied Ceramic Technology, 16(3), 981-993. https://doi.org/10.1111/ijac.13190
Related info:
- Version of
https://doi.org/10.1111/ijac.13190 - Version of
https://machinery.mas.bg.ac.rs/handle/123456789/3101
DOI: 10.1111/ijac.13190
ISSN: 1546-542X (Print); 1744-7402 (Online)
WoS: 000463236200011
Scopus: 2-s2.0-85061495283
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Institution/Community
Mašinski fakultetTY - JOUR AU - Nikolić, Maria Vesna AU - Vasiljević, Zorka Ž. AU - Luković, Miloljub D. AU - Pavlović, Vera P. AU - Krstić, Jugoslav B. AU - Vujančević, Jelena AU - Tadić, Nenad AU - Vlahović, Branislav AU - Pavlović, Vladimir B. PY - 2019 UR - https://machinery.mas.bg.ac.rs/handle/123456789/4066 AB - Zinc ferrite nanocrystalline powder was obtained by solid state synthesis of starting zinc oxide and hematite nanopowders. Field emission scanning electron microscopy (FESEM) and transmission electron microscopy (TEM), X‐ray diffraction (XRD), X‐ray photoelectron spectroscopy (XPS) and Raman spectroscopy confirmed the formation of nanocrystalline zinc‐ferrite powder with a mixed spinel structure with small amounts of remaining zinc oxide and hematite as impurities. Thick film paste was formed and screen printed on test interdigitated PdAg electrodes on alumina substrate. Formation of a porous nanocrystalline structure was confirmed by scanning electron microscopy (SEM) and Hg porosimetry. Humidity sensing properties of zinc ferrite thick films were investigated by monitoring the change in impedance in the relative humidity interval 30‐90% in the frequency range 42 Hz – 1 MHz at room temperature (25 °C) and 50 °C. At 42 Hz at both analyzed temperatures the impedance reduced ~ 46 times in the humidity range 30‐90%. The dominant influence of grain boundaries was confirmed by analysis of complex impedance with an equivalent circuit. PB - Wiley T2 - International Journal of Applied Ceramic Technology T1 - Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing EP - 993 IS - 3 SP - 981 VL - 16 DO - 10.1111/ijac.13190 ER -
@article{ author = "Nikolić, Maria Vesna and Vasiljević, Zorka Ž. and Luković, Miloljub D. and Pavlović, Vera P. and Krstić, Jugoslav B. and Vujančević, Jelena and Tadić, Nenad and Vlahović, Branislav and Pavlović, Vladimir B.", year = "2019", abstract = "Zinc ferrite nanocrystalline powder was obtained by solid state synthesis of starting zinc oxide and hematite nanopowders. Field emission scanning electron microscopy (FESEM) and transmission electron microscopy (TEM), X‐ray diffraction (XRD), X‐ray photoelectron spectroscopy (XPS) and Raman spectroscopy confirmed the formation of nanocrystalline zinc‐ferrite powder with a mixed spinel structure with small amounts of remaining zinc oxide and hematite as impurities. Thick film paste was formed and screen printed on test interdigitated PdAg electrodes on alumina substrate. Formation of a porous nanocrystalline structure was confirmed by scanning electron microscopy (SEM) and Hg porosimetry. Humidity sensing properties of zinc ferrite thick films were investigated by monitoring the change in impedance in the relative humidity interval 30‐90% in the frequency range 42 Hz – 1 MHz at room temperature (25 °C) and 50 °C. At 42 Hz at both analyzed temperatures the impedance reduced ~ 46 times in the humidity range 30‐90%. The dominant influence of grain boundaries was confirmed by analysis of complex impedance with an equivalent circuit.", publisher = "Wiley", journal = "International Journal of Applied Ceramic Technology", title = "Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing", pages = "993-981", number = "3", volume = "16", doi = "10.1111/ijac.13190" }
Nikolić, M. V., Vasiljević, Z. Ž., Luković, M. D., Pavlović, V. P., Krstić, J. B., Vujančević, J., Tadić, N., Vlahović, B.,& Pavlović, V. B.. (2019). Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing. in International Journal of Applied Ceramic Technology Wiley., 16(3), 981-993. https://doi.org/10.1111/ijac.13190
Nikolić MV, Vasiljević ZŽ, Luković MD, Pavlović VP, Krstić JB, Vujančević J, Tadić N, Vlahović B, Pavlović VB. Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing. in International Journal of Applied Ceramic Technology. 2019;16(3):981-993. doi:10.1111/ijac.13190 .
Nikolić, Maria Vesna, Vasiljević, Zorka Ž., Luković, Miloljub D., Pavlović, Vera P., Krstić, Jugoslav B., Vujančević, Jelena, Tadić, Nenad, Vlahović, Branislav, Pavlović, Vladimir B., "Investigation of ZnFe2O4 spinel ferrite nanocrystalline screen-printed thick films for application in humidity sensing" in International Journal of Applied Ceramic Technology, 16, no. 3 (2019):981-993, https://doi.org/10.1111/ijac.13190 . .