Determination of Mechanical Properties of Epoxy Composite Materials Reinforced with Silicate Nanofillers Using Digital Image Correlation (DIC)
2022
Autori
Jelić, AleksandraSekulić, Milica
Travica, Milan
Grzetić, Jelena
Ugrinović, Vukašin
Marinković, Aleksandar D.
Bozić, Aleksandra
Stamenović, Marina
Putić, Slaviša
Članak u časopisu (Objavljena verzija)
Metapodaci
Prikaz svih podataka o dokumentuApstrakt
In this study, silicate nanofillers; dicalcium silicate, magnesium silicate, tricalcium silicate, and wollastonite; were synthesized using four different methods and incorporated into the epoxy resin to improve its mechanical properties. Characterization of the newly synthesized nanofillers was performed using Fourier-transformation infrared (FTIR) spectroscopy, X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The purpose of this study was to analyze newly developed composite materials reinforced with silicate nanoparticles utilizing tensile testing and a full-field non-contact 3D Digital Image Correlation (DIC) method. Analysis of deformation and displacement fields gives precise material behavior during testing. Testing results allowed a more reliable assessment of the structural integrity of epoxy composite materials reinforced using different silicate nanofillers. It was concluded that the addition of 3% of dicalcium silicate,... magnesium silicate, tricalcium silicate, and wollastonite lead to the increasement of tensile strength up to 31.5%, 29.0%, 27.5%, and 23.5% in comparison with neat epoxy, respectively. In order to offer more trustworthy information about the viscoelastic behavior of neat epoxy and composites, a dynamic mechanical analysis (DMA) was also performed and rheological measurements of uncured epoxy matrix and epoxy suspensions were obtained.
Ključne reči:
tensile properties / silicate nanofillers / epoxy resin / DMA / 3D DICIzvor:
Polymers, 2022, 14, 6Izdavač:
- MDPI, Basel
Finansiranje / projekti:
- Ministarstvo nauke, tehnološkog razvoja i inovacija Republike Srbije, institucionalno finansiranje - 200325 (Vojnotehnički institut - VTI, Beograd) (RS-MESTD-inst-2020-200325)
DOI: 10.3390/polym14061255
ISSN: 2073-4360
PubMed: 35335585
WoS: 000774485900001
Scopus: 2-s2.0-85127539303
Institucija/grupa
Inovacioni centarTY - JOUR AU - Jelić, Aleksandra AU - Sekulić, Milica AU - Travica, Milan AU - Grzetić, Jelena AU - Ugrinović, Vukašin AU - Marinković, Aleksandar D. AU - Bozić, Aleksandra AU - Stamenović, Marina AU - Putić, Slaviša PY - 2022 UR - https://machinery.mas.bg.ac.rs/handle/123456789/3775 AB - In this study, silicate nanofillers; dicalcium silicate, magnesium silicate, tricalcium silicate, and wollastonite; were synthesized using four different methods and incorporated into the epoxy resin to improve its mechanical properties. Characterization of the newly synthesized nanofillers was performed using Fourier-transformation infrared (FTIR) spectroscopy, X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The purpose of this study was to analyze newly developed composite materials reinforced with silicate nanoparticles utilizing tensile testing and a full-field non-contact 3D Digital Image Correlation (DIC) method. Analysis of deformation and displacement fields gives precise material behavior during testing. Testing results allowed a more reliable assessment of the structural integrity of epoxy composite materials reinforced using different silicate nanofillers. It was concluded that the addition of 3% of dicalcium silicate, magnesium silicate, tricalcium silicate, and wollastonite lead to the increasement of tensile strength up to 31.5%, 29.0%, 27.5%, and 23.5% in comparison with neat epoxy, respectively. In order to offer more trustworthy information about the viscoelastic behavior of neat epoxy and composites, a dynamic mechanical analysis (DMA) was also performed and rheological measurements of uncured epoxy matrix and epoxy suspensions were obtained. PB - MDPI, Basel T2 - Polymers T1 - Determination of Mechanical Properties of Epoxy Composite Materials Reinforced with Silicate Nanofillers Using Digital Image Correlation (DIC) IS - 6 VL - 14 DO - 10.3390/polym14061255 ER -
@article{ author = "Jelić, Aleksandra and Sekulić, Milica and Travica, Milan and Grzetić, Jelena and Ugrinović, Vukašin and Marinković, Aleksandar D. and Bozić, Aleksandra and Stamenović, Marina and Putić, Slaviša", year = "2022", abstract = "In this study, silicate nanofillers; dicalcium silicate, magnesium silicate, tricalcium silicate, and wollastonite; were synthesized using four different methods and incorporated into the epoxy resin to improve its mechanical properties. Characterization of the newly synthesized nanofillers was performed using Fourier-transformation infrared (FTIR) spectroscopy, X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM). The purpose of this study was to analyze newly developed composite materials reinforced with silicate nanoparticles utilizing tensile testing and a full-field non-contact 3D Digital Image Correlation (DIC) method. Analysis of deformation and displacement fields gives precise material behavior during testing. Testing results allowed a more reliable assessment of the structural integrity of epoxy composite materials reinforced using different silicate nanofillers. It was concluded that the addition of 3% of dicalcium silicate, magnesium silicate, tricalcium silicate, and wollastonite lead to the increasement of tensile strength up to 31.5%, 29.0%, 27.5%, and 23.5% in comparison with neat epoxy, respectively. In order to offer more trustworthy information about the viscoelastic behavior of neat epoxy and composites, a dynamic mechanical analysis (DMA) was also performed and rheological measurements of uncured epoxy matrix and epoxy suspensions were obtained.", publisher = "MDPI, Basel", journal = "Polymers", title = "Determination of Mechanical Properties of Epoxy Composite Materials Reinforced with Silicate Nanofillers Using Digital Image Correlation (DIC)", number = "6", volume = "14", doi = "10.3390/polym14061255" }
Jelić, A., Sekulić, M., Travica, M., Grzetić, J., Ugrinović, V., Marinković, A. D., Bozić, A., Stamenović, M.,& Putić, S.. (2022). Determination of Mechanical Properties of Epoxy Composite Materials Reinforced with Silicate Nanofillers Using Digital Image Correlation (DIC). in Polymers MDPI, Basel., 14(6). https://doi.org/10.3390/polym14061255
Jelić A, Sekulić M, Travica M, Grzetić J, Ugrinović V, Marinković AD, Bozić A, Stamenović M, Putić S. Determination of Mechanical Properties of Epoxy Composite Materials Reinforced with Silicate Nanofillers Using Digital Image Correlation (DIC). in Polymers. 2022;14(6). doi:10.3390/polym14061255 .
Jelić, Aleksandra, Sekulić, Milica, Travica, Milan, Grzetić, Jelena, Ugrinović, Vukašin, Marinković, Aleksandar D., Bozić, Aleksandra, Stamenović, Marina, Putić, Slaviša, "Determination of Mechanical Properties of Epoxy Composite Materials Reinforced with Silicate Nanofillers Using Digital Image Correlation (DIC)" in Polymers, 14, no. 6 (2022), https://doi.org/10.3390/polym14061255 . .